Rapid Sample Enrichment, Novel Derivatization, and High Sensitivity for Determination of 3-Chloropropane-1,2-diol in Soy Sauce via High-Performance Liquid Chromatography-Tandem Mass Spectrometry.

Soy Foods / analysis alpha-Chlorohydrin / analysis Tandem Mass Spectrometry Gas Chromatography-Mass Spectrometry / methods Chromatography, High Pressure Liquid Carbon
3-MCPD HPLC-MS/MS acid-hydrolyzed vegetable protein carbon yarn facile derivatization food contaminant p-(dimethylamino)-phenol

Journal

Journal of agricultural and food chemistry
ISSN: 1520-5118
Titre abrégé: J Agric Food Chem
Pays: United States
ID NLM: 0374755

Informations de publication

Date de publication:
18 Oct 2023
Historique:
medline: 23 10 2023
pubmed: 5 10 2023
entrez: 5 10 2023
Statut: ppublish

Résumé

A novel, simplified derivatization method and a rapid sample preparation process using carbon yarn as a sorbent for the determination of 3-chloropropane-1,2-diol (3-MCPD) in soy sauce via high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) was developed. 3-MCPD was first enriched and purified with carbon yarn and then eluted with a methanol-water solution. Subsequently, the analyte underwent derivatization with

Identifiants

DOI: 10.1021/acs.jafc.3c05230 PMID: 37797339
pubmed: 37797339
doi: 10.1021/acs.jafc.3c05230
doi:

Substances chimiques

alpha-Chlorohydrin 96-24-2
Carbon 7440-44-0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

15388-15397

Auteurs

Yunyu Tang (Y)

Key Laboratory of Control of Quality and Safety for Aquatic Products, Ministry of Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Jungong 300, Shanghai 200090, P. R. China.

Guangxin Yang (G)

Key Laboratory of Control of Quality and Safety for Aquatic Products, Ministry of Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Jungong 300, Shanghai 200090, P. R. China.

Xiaoxia Liu (X)

School of Chemical and Environmental Engineering, Shanghai Institute of Technology, 100 Haiquan Road, Shanghai 201418, P. R. China.

Lixia Qin (L)

School of Chemical and Environmental Engineering, Shanghai Institute of Technology, 100 Haiquan Road, Shanghai 201418, P. R. China.

Wenlei Zhai (W)

Institute of Quality Standard and Testing Technology, Beijing Academy of Agriculture and Forestry Sciences, Beijing 100097, P. R. China.

Essy Kouadio Fodjo (EK)

Laboratory of Constitution and Reaction of Matter, UFR SSMT, Université Felix Houphouet Boigny, Abidjan 22 22 BP 582, Cote d'Ivoire.
ORCID: 0000-0002-7915-7216

Xiaosheng Shen (X)

Key Laboratory of Control of Quality and Safety for Aquatic Products, Ministry of Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Jungong 300, Shanghai 200090, P. R. China.

Yuan Wang (Y)

Key Laboratory of Control of Quality and Safety for Aquatic Products, Ministry of Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Jungong 300, Shanghai 200090, P. R. China.

Xiaoyi Lou (X)

Key Laboratory of Control of Quality and Safety for Aquatic Products, Ministry of Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Jungong 300, Shanghai 200090, P. R. China.

Cong Kong (C)

Key Laboratory of Control of Quality and Safety for Aquatic Products, Ministry of Agriculture and Rural Affairs, East China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Jungong 300, Shanghai 200090, P. R. China.
ORCID: 0000-0001-8084-2133

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Classifications MeSH

questionsmedicales.fr › Aliments et boissons › Aliments › Légumes › Produits à base de légumes › Produits alimentaires à base de soja › Rapid Sample Enrichment, Novel Derivatization,...
questionsmedicales.fr › Composés chimiques organiques › Alcools › Glycols › Propylène glycols › alpha-Chlorohydrine › Rapid Sample Enrichment, Novel Derivatization,...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Spectrométrie de masse en tandem › Rapid Sample Enrichment, Novel Derivatization,...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Chromatographie gazeuse-spectrométrie de masse › Rapid Sample Enrichment, Novel Derivatization,...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Chromatographie en phase liquide à haute performance › Rapid Sample Enrichment, Novel Derivatization,...
questionsmedicales.fr › Produits chimiques inorganiques › Éléments › Carbone › Rapid Sample Enrichment, Novel Derivatization,...