Liquid phase microextraction based on natural deep eutectic solvents of psychoactive substances from biological fluids and natural waters.


Journal

Talanta
ISSN: 1873-3573
Titre abrégé: Talanta
Pays: Netherlands
ID NLM: 2984816R

Informations de publication

Date de publication:
15 Jan 2024
Historique:
received: 28 06 2023
revised: 28 09 2023
accepted: 04 10 2023
medline: 9 11 2023
pubmed: 10 10 2023
entrez: 9 10 2023
Statut: ppublish

Résumé

In this paper, natural deep eutectic solvents (NADES)-based for liquid phase microextraction (LPME) is proposed for the isolation of different psychoactive substances in water and biological fluids followed by liquid chromatography-tandem mass spectrometry (LC-MS/MS). The NADES composition was optimized (L-menthol:octanoic acid, 1:2 M ratio) prior to the study of the extraction conditions such as sample and elution volumes, obtaining up to 16-fold preconcentration factor. Next, the quality parameters were studied including linearity from LOQs (0.0006-0.05 μg L

Identifiants

pubmed: 37813012
pii: S0039-9140(23)01028-7
doi: 10.1016/j.talanta.2023.125277
pii:
doi:

Substances chimiques

Deep Eutectic Solvents 0
Solvents 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

125277

Informations de copyright

Copyright © 2023 The Authors. Published by Elsevier B.V. All rights reserved.

Déclaration de conflit d'intérêts

Declaration of competing interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Auteurs

Patricia García-Atienza (P)

Department of Analytical Chemistry, University of Valencia, Dr Moliner 50, 46100, Burjassot, Valencia, Spain.

Héctor Martínez-Pérez-Cejuela (H)

Department of Analytical Chemistry, University of Valencia, Dr Moliner 50, 46100, Burjassot, Valencia, Spain.

José Manuel Herrero-Martínez (J)

Department of Analytical Chemistry, University of Valencia, Dr Moliner 50, 46100, Burjassot, Valencia, Spain.

Sergio Armenta (S)

Department of Analytical Chemistry, University of Valencia, Dr Moliner 50, 46100, Burjassot, Valencia, Spain. Electronic address: sergio.armenta@uv.es.

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Classifications MeSH